お知らせ • Jul 24
CleanTech Lithium Produces High Purity Lithium Carbonate And Undertakes Optimisation Work
CleanTech Lithium announced the results of the processing of eluate produced by the Company's DLE pilot plant in Chile into approximately 330kg of high purity lithium carbonate. This downstream processing was undertaken by USA based, vertically integrated lithium production and technology company, Empower EIT (Empower). Empower processed approximately 55,000 litres of eluate at its advanced lithium processing facility in Dallas, USA. The eluate was produced from Laguna Verde brine at CleanTech Lithium´s DLE pilot plant located in Copiapó, Chile. 330kg of lithium carbonate has been produced by Empower with laboratory results showing a lithium carbonate purity ranging across five campaigns from 99.68% to 99.91% in the final campaign. An additional approximately 250kg of lithium carbonate is stored in recycle fluids from pre-treatment and carbonation. The nanofiltration stage utilised the latest DuPont™ FilmTec™ LiNE-XD Element high productivity nanofiltration membranes for lithium brine purification to achieve superior purification and efficiency. Other key process and project studies are currently underway: a PFS process validation trial in Chile, definitive feasibility study (DFS) level adsorbent test-work in France, and a spent brine reinjection option study. Empower provides a fully USA-based end-to-end lithium processing solution at its new 1600m2 facility based in Dallas, Texas, where processing commenced on 55,000 litres of eluate between March and May 2026. The primary objective was to demonstrate the process can consistently produce lithium carbonate product. The nano-filtration unit containing DuPont™ LiNE-XD 4040 membranes contributed to an excellent reduction in calcium and magnesium present in the eluate. Boron was then removed by Ion-Exchange (IX). Under optimised continuous operating conditions, the Empower conversion platform achieved approximately 97% boron removal. Residual boron was subsequently concentrated in the thermal evaporation stage requiring additional downstream polishing. Final polishing successfully reduced boron concentrations prior to carbonation. Boron is the primary contaminant requiring removal in the post DLE downstream processing. The Company will evaluate the potential for the removed boron to be a by-product that enhances project economics. The process was run in a continuous fashion up until the carbonation stage, which used batch processing. Five carbonation batches were produced which in addition to producing solid lithium carbonate also produced a volume of carbonation liquor or lithium rich permeate, which is retained for reprocessing and lithium recovery. Carbonation and polishing produced high purity lithium carbonate of >99.7% purity. Independent laboratory results undertaken at Benchmark Laboratory, Houston, USA, were received for batches 1 through 5 as presented in Table 1. The results confirm the production of a high purity product. Batch 1: Li2CO3 99.76%, Ca 0.01%, Mg 0.01%, Na 0.10%, K 0.02%, B 0.05%, Ni 0.00%, Cl 0.00%, Si 0.05%, S 0.00%, P 0.00%. Batch 2: Li2CO3 99.68%, Ca 0.01%, Mg 0.01%, Na 0.26%, K 0.03%, B 0.01%, Ni 0.00%, Cl 0.00%, Si 0.01%, S 0.00%, P 0.00%. Batch 3: Li2CO3 99.85%, Ca 0.01%, Mg 0.01%, Na 0.09%, K 0.02%, B 0.01%, Ni 0.00%, Cl 0.01%, Si 0.00%, S 0.01%, P 0.00%. Batch 4: Li2CO3 99.86%, Ca 0.02%, Mg 0.02%, Na 0.00%, K 0.00%, B 0.00%, Ni 0.03%, Cl 0.00%, Si 0.03%, S 0.05%, P 0.00%. Batch 5: Li2CO3 99.91%, Ca 0.02%, Mg 0.02%, Na 0.00%, K 0.00%, B 0.00%, Ni 0.03%, Cl 0.00%, Si 0.02%, S 0.00%, P 0.00%. The Company is undertaking a pilot programme with Xian Lanshen New Material Company (Lanshen) to optimise and verify the process utilised in the PFS for the Laguna Verde project. A volume of 20m3 of feed brine from Laguna Verde is being processed at Lanshen´s pilot plant facility in Santiago, Chile. Reports have been received on the first stage to verify DLE process parameters, and the second stage of evaluating advanced membrane and purification process steps. The final stage is carbonation to lithium carbonate to meet rigorous Chinese battery grade standards, including production of a 5kg sample of lithium carbonate. When the final stage is completed and the lithium carbonate sample tested by an external laboratory, the results will be reported to the market. An adsorbent trial will commence in the coming weeks, once material transfer is completed, in collaboration with French consulting firm Hephaistos Insights to conduct Direct Lithium Extraction (DLE) benchmarking and eluate analysis using brine from Laguna Verde. The programme will assess a range of adsorbent options against the project's specific brine chemistry, with a particular focus on elution efficiency. The bench-scale testing, which will be executed by specialist subcontractor Seprosys SAS, will include the Company's current reference adsorbent alongside alternatives from North American and European suppliers. This workstream is designed to confirm the optimal adsorbent selection for Laguna Verde ahead of the DFS. CTL has engaged Zelandez to conduct a comprehensive spent brine reinjection options analysis for the Laguna Verde project. Zelandez will deploy a multidisciplinary team of hydrogeologists, reservoir engineers, and DLE experts to evaluate aquifer reinjection concepts, culminating in a technical analysis that integrates vital basin-dynamics, environmental permitting screens, and CAPEX/OPEX modelling delivering a recommended DFS workplan to advance the project toward sustainable development.
